Ethylenediamine → HCID 66658225, compound

HRID 420858Notes

Reaction equation

HRID 420858 reaction equation
[N:1]1([C:6]2[CH:11]=[CH:10][C:9]([C:12](=O)[CH3:13])=[CH:8][CH:7]=2)[CH:5]=[N:4][N:3]=[N:2]1.[CH2:15]([NH2:18])[CH2:16][NH2:17]>C(O)(=O)C>[N:1]1([C:6]2[CH:11]=[CH:10][C:9]([CH:12]([NH:17][CH2:16][CH2:15][NH2:18])[CH3:13])=[CH:8][CH:7]=2)[CH:5]=[N:4][N:3]=[N:2]1

Participants

4

Reactant 2

HCID 3301EthylenediamineHCID 7164331-(4-Tetrazol-1-yl-phenyl)-ethanone

Product 1

HCID 66658225HCID 66658225, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

By using 1-[4-(1H-tetrazol-1-yl)phenyl]ethanone (250 mg), ethylenediamine (400 μl) and acetic acid (700 μl) as starting materials, the title compound (60.5 mg) was obtained in the same manner as that of Reference Example 64, (1).

Sources & evidence

ORD record
ord-721b887df42e46d68f3b0c2f7071a256
Source dataset
uspto-grants-2012_01
Patent number
US08097708B2

Reaction notes

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