2,5-Dichloroaniline → 5-Chloro-N-(2,5-dichlorophenyl)-2-hydroxybenzamide

HRID 421124Notes

Reaction equation

HRID 421124 reaction equation
[Cl:1][C:2]1[CH:10]=[C:6]([C:7]([OH:9])=O)[C:5]([OH:11])=[CH:4][CH:3]=1.[Cl:12][C:13]1[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][C:14]=1[NH2:15]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([OH:11])=[C:6]([CH:10]=1)[C:7]([NH:15][C:14]1[CH:16]=[C:17]([Cl:20])[CH:18]=[CH:19][C:13]=1[Cl:12])=[O:9]

Participants

3

Reactant 2

HCID 72622,5-DichloroanilineHCID 94475-Chlorosalicylic Acid

Product 1

HCID 129247115-Chloro-N-(2,5-dichlorophenyl)-2-hydroxybenzamideYield 10.8%

Procedure

Using 5-chlorosalicylic acid and 2,5-dichloroaniline as the raw materials, the same operation as the example 16 gave the title compound.

Sources & evidence

ORD record
ord-f1dc1b020a1647ca9d619be6094240d9
Source dataset
uspto-grants-2012_01
Patent number
US08097759B2

Reaction notes

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