Acetyl chloride → 2-Acetoxy-N-{3,5-bis[(1,1-dimethyl)ethyl]phenyl}-5-chlorobenzamide

Participants

Role	Name	HCID	Charge
Reactant	Acetyl chloride	HCID 6367	—
Reactant	5-chloro-N-(3,5-ditert-butylphenyl)-2-hydroxy-benzamide	HCID 66657148	—
Product	2-Acetoxy-N-{3,5-bis[(1,1-dimethyl)ethyl]phenyl}-5-chlorobenzamide	HCID 66657132	66.1%

Reaction Steps

Using N-{3,5-bis[(1,1-dimethyl)ethyl]phenyl}-5-chloro-2-hydroxybenzamide and acetyl chloride as the raw materials, the same operation as the example 96 gave the title compound.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08097759B2
Source dataset	uspto-grants-2012_01
ORD ID	ord-c21be64b3af14ac3b145edb646a0fb8c
Source note	uspto-grants-2012_01