HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67536381, compound → 7alpha-Formylandrostane-3,17-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67536381 | HCID 67536381 | — |
| Reactant | HCID 86635593 | HCID 86635593 | — |
| Product | 7alpha-Formylandrostane-3,17-dione | HCID 86635592 | 85% |
Reaction Steps
7α-Formylandrostane-3,17-dione was prepared in 85% yield from 3,3:17,17-bis(ethylendioxy)-7α-formylandrostane (2.36 g) by the procedure described above for the preparation of 6-methyleneandrostane-3,17-dione (II-ac, Prepn. 13). 1H-NMR (300 MHz, acetone-d6, ppm from TMS): δ 9.95 (1H, d), 2.57-0.80 (21H, m), 0.95 (3H, s), 0.80 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536160B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-c8c9487b74514d218f523c0f22b69599 |
| Source note | uspto-grants-2013_09 |