HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 421542Generated: November 2, 2026
Sodium Hydroxide → ZINC trans-styrylacetate
https://huagongshe.com/reaction/421542
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Zincchloride | HCID 3007855 | — |
| Reactant | 3-Butenoic acid, 4-phenyl-, (3E)- | HCID 5370625 | — |
| Solvent | Water | HCID 962 | — |
| Product | ZINC trans-styrylacetate | HCID 14438687 | 77.4% |
Reaction Steps
A solution of 47% (w/w) sodium hydroxide (5.5 g) is added to slurry of trans-styrylacetic acid (8.1 g, 0.05 mol) in water (100 mL) at 70° C. to give a clear slightly alkaline solution. A solution of zinc chloride (3.4 g, 0.025 mol) in water (50 mL) is added and a precipitate is formed immediately. The mixture is stirred at 70° C. for further 2.5 hours. The precipitate is then filtered and dried to yield 7.5 g (77%) zinc trans-styrylacetate as a fine white powder. IR absorption bands: 1526, 1436 and 1385 cm−1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08101544B2 |
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| Source dataset | uspto-grants-2012_01 |
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| ORD ID | ord-64e82efa25e248b0a93352064a29df91 |
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| Source note | uspto-grants-2012_01 |
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