HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10857231, compound → HCID 86609651, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10857231 | HCID 10857231 | — |
| Reactant | N~2~-(tert-Butoxycarbonyl)-N-methoxy-N-methyl-D-alaninamide | HCID 23537239 | — |
| Product | HCID 86609651 | HCID 86609651 | 79% |
Reaction Steps
The title compound was prepared as Methyl (2E)(4S)-4-[(tert-butoxy)carbonylamino]pent-2-enoate with (2R)-2-[(tert-butoxy)carbonylamino]-N-methoxy-N-methylpropanamide (13.05 grams, 56.18 mmol) to give the title compound (10.2 g, 79%): ES-MS (m/z) 230 [M+1]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101588B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-e0e4fd5fa9ff410f9c3c13ccb1874126 |
| Source note | uspto-grants-2012_01 |