HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-4-fluorobenzoic acid → HCID 16730712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-4-fluorobenzoic acid | HCID 520989 | — |
| Reactant | N-(3-amino-4-chlorophenyl)-2-methyl-6-(trifluoromethyl)nicotinamide | HCID 16730560 | — |
| Product | HCID 16730712 | HCID 16730712 | — |
Reaction Steps
N-(3-amino-4-chlorophenyl)-2-methyl-6-(trifluoromethyl)nicotinamide (0.15 mmol) was used in general procedure 2 with 3-chloro-4-fluorobenzoic acid (0.167 mmol). The product was purified by RP-HPLC to give N-(4-chloro-3-(3-chloro-4-fluorobenzamido)phenyl)-2-methyl-6-(trifluoromethyl)nicotinamide. MS (Q1) 486.1 (M)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101610B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-de703f269632450884536f4d0c70a072 |
| Source note | uspto-grants-2012_01 |