HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N-(2-chloro-5-nitrophenyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 2-Chloro-5-nitroaniline | HCID 22691 | — |
| Product | N-(2-chloro-5-nitrophenyl)benzamide | HCID 779142 | — |
Reaction Steps
2-chloro-5-nitroaniline (Aldrich), (10.0 mmol) was used in general procedure 1 with benzoyl chloride (12.2 mmol). The product was purified by silica gel chromatography (40% EtOAc/Hex) to give N-(2-chloro-5-nitrophenyl)benzamide as a tan solid. MS (Q1) 276.1 (M)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101610B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-1a1cadeee3a543eea92bb60c3d4e0ea0 |
| Source note | uspto-grants-2012_01 |