N-(5-amino-2-chlorophenyl)benzamide → N-(3-benzamido-4-chlorophenyl)-1-(4-fluorophenyl)-4-methyl-1H-pyrazole-3-carboxamide

Participants

Role	Name	HCID	Charge
Reactant	N-(5-amino-2-chlorophenyl)benzamide	HCID 721122	—
Reactant	1-(4-fluorophenyl)-4-methyl-1H-pyrazole-3-carboxylic acid	HCID 66675928	—
Product	N-(3-benzamido-4-chlorophenyl)-1-(4-fluorophenyl)-4-methyl-1H-pyrazole-3-carboxamide	HCID 16730793	—

Reaction Steps

N-(5-amino-2-chlorophenyl)benzamide (0.24 mmol) was used in general procedure 2 with 1-(4-fluorophenyl)-4-methyl-1H-pyrazole-3-carboxylic acid (0.30 mmol). The product was purified by RP-HPLC to give N-(3-benzamido-4-chlorophenyl)-1-(4-fluorophenyl)-4-methyl-1H-pyrazole-3-carboxamide. MS (Q1) 449.1 (M)+

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08101610B2
Source dataset	uspto-grants-2012_01
ORD ID	ord-1b8f1622d43b48b7a9f305cbaecddde5
Source note	uspto-grants-2012_01