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HRID421692

反应详情

EQUATION

反应方程式

HRID 421692 的结构方程式

REACTANTS

反应物

2
结构：C[C@@H]1CNC[C@H](C)N1
HCID6950261

rel-(2R,6S)-2,6-Dimethylpiperazine

C6H14N2

结构：Cc1nc(Cl)ccc1C(=O)Nc1ccc(Cl)c(NC(=O)c2ccccc2)c1
HCID16730950

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ncccc1C(N)=O
HCID12243705

2-methylnicotinamide

C7H8N2O

PROCEDURE

实验过程

N-(3-benzamido-4-chlorophenyl)-6-chloro-2-methylnicotinamide (0.15 mmol) was used in general procedure 3 with cis-2,6-dimethylpiperazine (0.77 mmol). The product was purified by RP-HPLC to give N-(3-benzamido-4-chlorophenyl)-6-(3S-,5R)-3-5-dimethylpiperazine-1-yl)-2-methyl-nicotinamide. MS (Q1) 464.0 (M)+

WORKUP

后处理

  1. customThe product was purified by RP-HPLC