HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-(methylsulfonyl)benzoic acid → Nicotinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-(methylsulfonyl)benzoic acid | HCID 735863 | — |
| Reactant | N-(5-Amino-2-chlorophenyl)nicotinamide | HCID 28867202 | — |
| Product | Nicotinamide | HCID 936 | — |
Reaction Steps
N-(5-amino-2-chlorophenyl)nicotinamide (0.40 mmol) was used in general procedure 2 with 2-chloro-4-(methylsulfonyl)benzoic acid (0.48 mmol). The product was purified by RP-HPLC to give N-(2-chloro-4-(methylsulfonyl)benzamido)phenyl)nicotinamide. MS (Q1) 464.0 (M)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101610B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-1e1bd51e940d40f0a15ca1091c84de62 |
| Source note | uspto-grants-2012_01 |