HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-5-nitroaniline → 3-chloro-N-(2-chloro-5-nitrophenyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-5-nitroaniline | HCID 22691 | — |
| Reactant | Benzoyl chloride, 3-chloro- | HCID 69252 | — |
| Product | 3-chloro-N-(2-chloro-5-nitrophenyl)benzamide | HCID 871095 | — |
Reaction Steps
2-chloro-5-nitroaniline (Aldrich, 25.7 mmol) was used in general procedure 1 with 3-chlorobenzoyl chloride (26.5 mmol). The product was purified by silica gel chromatography (40% EtOAc/Hex) to give 3-chloro-N-(2-chloro-5-nitrophenyl)benzamide as a brown solid. MS (Q1) 294.0 (M)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101610B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-9144608349354df5b1026a8265d1d3cb |
| Source note | uspto-grants-2012_01 |