HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloro-3-pyridinecarbonitrile → HCID 44186115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloro-3-pyridinecarbonitrile | HCID 5152094 | — |
| Reactant | 1-benzyl-4-((S)-3-methyl-piperazin-1-yl)-phthalazine | HCID 44186479 | — |
| Product | HCID 44186115 | HCID 44186115 | 23% |
Reaction Steps
Following the above procedure, 6-chloro-nicotinonitrile (50 mg, 0.36 mmol, 1.2 eq) and 1-benzyl-4-((S)-3-methyl-piperazin-1-yl)-phthalazine (100 mg, 0.31 mmol, 1.0 eq) afford the title compound as a white solid (30 mg, 23% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536168B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-617f704358324342ba9d50efd5543e62 |
| Source note | uspto-grants-2013_09 |