HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromopyridine → HCID 11701908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromopyridine | HCID 7973 | — |
| Reactant | HCID 86086776 | HCID 86086776 | — |
| Product | HCID 11701908 | HCID 11701908 | 11.6% |
Reaction Steps
The title compound was prepared in accordance with the general method of Example 1, from 2-bromopyridine (15 mg, 97=mol) and 2-(but-3-ynyl)-4-chlorobenzo[d]oxazole (20 mg, 97 μmol). The crude residue was purified by flash chromatography (cyclohexane/AcOEt 4:1) to yield 3 mg (11 μmol, 11%) of 4-chloro-2-(4-(pyridin-2-yl)but-3-ynyl)benzo[d]oxazole as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101637B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-17a8e95c9cc6402dbe84a4f4c47a8635 |
| Source note | uspto-grants-2012_01 |