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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 422334Generated: October 29, 2026

2-Bromopyridine → HCID 66598012, compound

https://huagongshe.com/reaction/422334

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-BromopyridineHCID 7973—
ReactantHCID 86086874HCID 86086874—
ProductHCID 66598012HCID 6659801214.3%

Reaction Steps

The title compound was prepared in accordance with the general method of Example 1, from 2-bromopyridine (166 mg, 1.05 mmol) and 2-but-3-ynyl-4-chloro-benzo[d]thiazole (233 mg, 1.05 mmol). The crude residue was purified by flash chromatography (DCM/MeOH 99:1 to 98:2) to yield 46 mg (0.15 mmol, 14% o) of 4-chloro-2-(4-(pyridin-2-yl)but-3-ynyl)benzo[d]thiazole as a brown oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08101637B2
Source datasetuspto-grants-2012_01
ORD IDord-4faa6ba16ac1495e84e106a4423887ab
Source noteuspto-grants-2012_01