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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 422366Generated: October 28, 2026

2-Bromopyridine → HCID 66597894, compound

https://huagongshe.com/reaction/422366

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-BromopyridineHCID 7973—
Reactant5-Hexyn-1-olHCID 70234—
ProductHCID 66597894HCID 6659789478%

Reaction Steps

The title compound was prepared in accordance with the general method of Example 1, from 2-bromopyridine (6.44 g, 40.8 mmol) and hex-5-yn-1-ol (4.00 g, 40.8 mmol). The crude residue was purified by flash chromatography (DCM/MeOH 1:1) to yield 5.56 g (31.7 mmol, 78%) of 6-pyridin-2-yl-hex-5-yn-1-ol as an orange oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08101637B2
Source datasetuspto-grants-2012_01
ORD IDord-b98c616c5c7e4c6cadfb808e350c6ba5
Source noteuspto-grants-2012_01