HuagongsheHuagongshe Chemistry Print Report · For research reference only
1(2H)-Phthalazinone → 2-(6-(pyridin-2-yl)hex-5-ynyl)phthalazin-1(2H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1(2H)-Phthalazinone | HCID 8394 | — |
| Reactant | 2-(6-Bromohex-1-ynyl)pyridine | HCID 20331212 | — |
| Product | 2-(6-(pyridin-2-yl)hex-5-ynyl)phthalazin-1(2H)-one | HCID 66598667 | — |
Reaction Steps
The title compound was prepared in accordance with the general method of Example 242(B), from 2-(6-bromo-hex-1-ynyl)pyridine (138 mg, 0.578 mmol) and phthalazin-1(2H)-one (80 mg, 0.55 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101637B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-6c27de8cea214daeaa961f7050308de4 |
| Source note | uspto-grants-2012_01 |