HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 422548Generated: November 1, 2026
Potassium Carbonate → HCID 59726020, compound
https://huagongshe.com/reaction/422548
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Methylphenyl boronic acid | HCID 2733267 | — |
| Reactant | HCID 59726015 | HCID 59726015 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Solvent | Dimethoxyethane ethanol water | HCID 86587095 | — |
| Product | HCID 59726020 | HCID 59726020 | — |
Reaction Steps
A glass microwave reaction vessel was charged with 3-(1-chlorophthalazin-6-yl)-4-methyl-N-(1-methyl-1H-pyrazol-5-yl)benzamide (65 mg, 172 μmol), o-tolylboronic acid (28 mg, 206 μmol), potassium carbonate (31 μl 516 μmol), tetrakis(triphenylphosphine)palladium (20 mg, 17 μmol) and DME:water:ethanol (7:3:2, 2 mL). The reaction mixture was stirred and heated in a Smith Synthesizer® microwave reactor (Personal Chemistry, Inc., Upssala, Sweden) at 140° C. for 20 mins.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08101612B2 |
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| Source dataset | uspto-grants-2012_01 |
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| ORD ID | ord-2eb23926f1824510adfa8f1b632ecec8 |
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| Source note | uspto-grants-2012_01 |
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