Phenol → HCID 25267397, compound

Participants

Reaction Steps

The title compound 447 was synthesized from compound 33 (51 mg) using procedure F described for the synthesis of phenol 807. Yield: 31 mg (77%). 1H-NMR (400 MHz, CDCl3): δ ppm 7.14-7.07 (m, 2H), 6.93 (ddd, J=10.68, 8.09, 1.20 Hz, 1H), 6.78 (dt, J=8.02, 7.80, 4.33 Hz, 1H), 6.74-6.68 (m, 3H), 5.00 (dd, J=7.26, 1.60 Hz, 1H), 4.95 (s, 1H), 2.40-2.28 (m, 1H), 2.22 (td, J=14.78, 7.49, 7.49 Hz, 1H), 2.14-2.04 (m, 1H), 1.86 (tdd, J=14.64, 12.73, 1.56, 1.56 Hz, 1H), 1.78-1.49 (m, 4H), 1.16-0.96 (m, 1H), 1.43-1.29 (m, 1H)

Provenance & Evidence