HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyloxonium tetrafluoroborate → HCID 178444700, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyloxonium tetrafluoroborate | HCID 2723982 | — |
| Reactant | HCID 178444699 | HCID 178444699 | — |
| Product | HCID 178444700 | HCID 178444700 | 100% |
Reaction Steps
2.09 g (11.01 mmol) of triethyloxonium tetrafluoroborate are added to 2.21 g (10.90 mmol) of 1-hexyl-3-methylimidazolium chloride. The reaction mixture is stirred at room temperature for 30 minutes, and all volatile products are subsequently removed over the course of 30 minutes in a vacuum of 13.3 Pa and at 80° C. (temperature of the oil bath), giving 2.77 g of 1-hexyl-3-methylimidazolium tetrafluoroborate as liquid. The yield is approximately quantitative.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101749B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-e0544f1efe0f4e1eb8073ab6c96e7e51 |
| Source note | uspto-grants-2012_01 |