HRID4237

反应详情

EQUATION

反应方程式

HRID 4237 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

0.11 mole (22.8 g) of 4,5-dichloro-2-nitroaniline is added to a solution of 0.55 mole (33.3 ml) of ethanolamine in 70 ml of dioxane. The reaction mixture is heated for 6 hours in refluxing dioxane. After dilution with water and neutralization with concentrated hydrochloric acid, the expected product precipitates.

WORKUP

后处理

  1. temperatureThe reaction mixture is heated for 6 hours
  2. customAfter dilution with water and neutralization with concentrated hydrochloric acid, the expected product precipitates