HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dinitro(trifluoromethoxy)benzene → 4-(Trifluoromethoxy)benzene-1,3-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dinitro(trifluoromethoxy)benzene | HCID 2737131 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 4-(Trifluoromethoxy)benzene-1,3-diamine | HCID 24902286 | — |
Reaction Steps
4-Trifluoromethoxy-benzene-1,3-diamine (D-4) was synthesized following the general scheme above starting from 2,4-dinitro-1-trifluoromethoxy-benzene. Yield (89%). HPLC ret. time 0.91 min, 10-99% CH3CN, 5 min run; ESI-MS 193.3 m/z (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101767B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-50d602bfbba94b9cbda47d61f473ac6f |
| Source note | uspto-grants-2012_01 |