HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 25205685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 57567368 | HCID 57567368 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 25205685 | HCID 25205685 | — |
Reaction Steps
[7-[(4-Oxo-1H-quinolin-3-yl)carbonylamino]tetralin-1-yl]aminoformic acid ethyl ester (482) was synthesized following the general scheme above, from amine (273-I) and ethyl chloroformate. Overall yield (18%). HPLC ret. time 2.84 min, 10-99% CH3CN, 5 min run; ESI-MS 406.5 m/z (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08101767B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-8bbbde7d292b49c1913c5ff553db778a |
| Source note | uspto-grants-2012_01 |