2-Bromobenzyl alcohol → 1-Bromo-2-((methoxymethoxy)methyl)benzene

HRID 424359Notes

Reaction equation

HRID 424359 reaction equation
BrC1C=CC=CC=1CO.[Br:10][C:11]1[CH:16]=[CH:15][C:14](F)=[CH:13][C:12]=1[CH2:18][O:19][CH2:20][O:21][CH3:22]>>[Br:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=1[CH2:18][O:19][CH2:20][O:21][CH3:22]

Participants

3

Reactant 2

HCID 728502-Bromobenzyl alcoholHCID 118455732-Bromo-5-fluoro-[1-(methoxymethoxy)methyl]benzene

Product 1

HCID 118459381-Bromo-2-((methoxymethoxy)methyl)benzene

Procedure

This compound was made from 2-bromobenzylalcohol in the same manner as compound 5b and used for the next step without purification.

Workup

  1. customused for the next step without purification

Sources & evidence

ORD record
ord-fd65769a8306421ea6f782e138d6bac7
Source dataset
uspto-grants-2012_01
Patent number
US08106031B2

Reaction notes

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