HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-4,5-difluorobenzoic acid → 2-Bromo-4,5-difluoro-1-(methoxymethoxymethyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-4,5-difluorobenzoic acid | HCID 2782789 | — |
| Reactant | 2-Bromo-5-chloro-1-(methoxymethoxymethyl)benzene | HCID 59024677 | — |
| Product | 2-Bromo-4,5-difluoro-1-(methoxymethoxymethyl)benzene | HCID 66704680 | — |
Reaction Steps
This compound was made from 2-bromo-4,5-difluorobenzoic acid in the same manner as compound 18d: 1H NMR (300 MHz, CDCl3) δ (ppm) 3.42 (s, 3H), 4.57 (d, J=1.2 Hz, 2H), 4.76 (s, 2H), 7.3-7.5 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106031B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-9dbc7819d0174dbbbca588c2ec68a961 |
| Source note | uspto-grants-2012_01 |