M-Phenylenediamine → N-[3-(4-Methoxyphenyl)-[1,2,4]triazolo[3,4-a]phthalazin-6-yl]benzene-1,3-diamine

HRID 424406Notes

Reaction equation

HRID 424406 reaction equation
Cl[C:2]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[C:5]2=[N:12][N:13]=[C:14]([C:15]3[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[CH:17][CH:16]=3)[N:4]2[N:3]=1.[C:23]1([NH2:30])[CH:28]=[CH:27][CH:26]=[C:25]([NH2:29])[CH:24]=1>>[CH3:22][O:21][C:18]1[CH:19]=[CH:20][C:15]([C:14]2[N:4]3[N:3]=[C:2]([NH:29][C:25]4[CH:26]=[CH:27][CH:28]=[C:23]([NH2:30])[CH:24]=4)[C:11]4[C:6]([C:5]3=[N:12][N:13]=2)=[CH:7][CH:8]=[CH:9][CH:10]=4)=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 7935M-PhenylenediamineHCID 7126896-Chloro-3-(4-methoxyphenyl)-[1,2,4]triazolo[3,4-a]phthalazine2×

Product 1

HCID 66703836N-[3-(4-Methoxyphenyl)-[1,2,4]triazolo[3,4-a]phthalazin-6-yl]benzene-1,3-diamine

Procedure

Starting from 6-chloro-3-(4-methoxy-phenyl)-[1,2,4]triazolo[3,4-a]phthalazine (compound B1) and m-phenylene-diamine, the title compound can be obtained analogously to one of the procedures as described for compound A1.

Sources & evidence

ORD record
ord-6ddcf1f8dc0a441488ca35223af7ff06
Source dataset
uspto-grants-2012_01
Patent number
US08106047B2

Reaction notes

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