HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → 5-(3-(Cyclopentyloxy)-4-methoxyphenyl)-2,6-dimethylpyridazin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | Veratraldehyde | HCID 8419 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 3-Cyclopentyloxy-4-methoxybenzaldehyde | HCID 2735893 | — |
| Reactant | Methylmethylsulfinylmethyl sulfide | HCID 54140058 | — |
| Product | 5-(3-(Cyclopentyloxy)-4-methoxyphenyl)-2,6-dimethylpyridazin-3-one | HCID 25128635 | — |
Reaction Steps
Using a method similar to Working Example 1 (1)-(4), 3-(cyclopentyloxy)-4-methoxybenzaldehyde was substituted for 3,4-dimethoxybenzaldehyde, methyl(1-methylsulfinyl)ethyl)sulfine for methyl methylsulfinyl-methylsulfide, and methylhydrazine for hydrazine hydrate to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106053B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-185336011efe4cb8a90b0415053b5dc4 |
| Source note | uspto-grants-2012_01 |