HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → 1-Piperidinesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Sulfamide | HCID 82267 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 1-Piperidinesulfonamide | HCID 276741 | — |
Reaction Steps
Piperidine (3.0 g) and sulfamide (5.93 g) in 1,4-dioxane (100 ml) were heated at reflux for 24 h. The solvent was evaporated under reduced pressure and the resulting solid suspended in CHCl3. The suspension was filtered and the filtrate concentrated in vacuo to afford the subtitle compound as a white solid. Yield: 3.85 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106063B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-ee0d5e1762a847a1929db3d27db38938 |
| Source note | uspto-grants-2012_01 |