HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 86602824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Methanesulfonamide | HCID 72879 | — |
| Reactant | 2-Chloromethyl 2-(trimethylsilyl)ethyl ether | HCID 2724271 | — |
| Reactant | HCID 85927872 | HCID 85927872 | — |
| Product | HCID 86602824 | HCID 86602824 | — |
Reaction Steps
The subtitle compound was prepared as a colourless oil by the method of Example 39 step iii) using the subtitle product of step v) (2.0 g), methanesulfonamide (0.60 g), 60% sodium hydride (0.50 g) and 2-(trimethylsilyl)ethoxymethyl chloride (1.11 ml). Yield: 2.42 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106063B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-f055446350f14757980bb0e662fb4b61 |
| Source note | uspto-grants-2012_01 |