HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 59263170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2,4-Dibenzyloxy-5-isopropyl-benzoic acid | HCID 59167879 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59263170 | HCID 59263170 | — |
Reaction Steps
2,4-Bis-benzyloxy-5-isoproyl-benzoic acid (0.2 g, 0.53 mmol) was dissolved in DCM (10 ml) and treated with oxalyl chloride (1.5 g, 12 mmol) and a catalytic amount of DMF. Stir reaction mixture at room temperature for 14 hours. Solvent was removed in vacuo. The crude material was dissolved in toluene and evaporated. Crude 2,4-bis-benzyloxy-5-isopropyl-benzoyl chloride was obtained as oil (200 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106057B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-51e5ceb0b9344b82af027f35dde22495 |
| Source note | uspto-grants-2012_01 |