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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 425463Generated: October 29, 2026

Isatin → HCID 66642639, compound

https://huagongshe.com/reaction/425463

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIsatinHCID 7054—
Reactant1-BromopentaneHCID 8057—
Reactant4-BromoindoleHCID 676494—
ReactantBenzyl 3-Bromopropyl EtherHCID 2776064—
ProductHCID 66642639HCID 66642639—

Reaction Steps

Following the procedure as described in PREPARATION 1A, and making non-critical variations to replace 4-bromoindole with isatin, and 1-bromopentane with benzyl 3-bromopropyl ether, the title compound was obtained (95%) as a pale yellow syrup: 1H NMR (300 MHz, CDCl3) δ 7.57-6.92 (m, 9H), 4.50 (s, 2H), 3.84 (t, 2H), 3.54 (t, 2H), 2.03-1.94 (m, 2H); MS (ES+) m/z 296.3 (M+1), 318.3 (M+23).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08106087B2
Source datasetuspto-grants-2012_01
ORD IDord-39c47ae59ec24befb9a2c39b5a1c531f
Source noteuspto-grants-2012_01