HRID425515

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID68289

Sesamol

C7H6O3

结构：O=C1C(=O)N(C(c2ccccc2)c2ccccc2)c2ccccc21

HCID1969277

1-(diphenylmethyl)-1H-indole-2,3-dione

C21H15NO2

HCID11126311

2,3-dihydrobenzofuran-5-ol

C8H8O2

HCID65596570

1-(2-cyclopropylethyl)-1H-indole-2,3-dione

C13H13NO2

PRODUCTS

生成物

结构：O=C1N(C(c2ccccc2)c2ccccc2)c2ccccc2C1(O)c1cc2c(cc1O)CCO2

HCID12004250

未命名化合物

PROCEDURE

实验过程

Following the procedure as described in PREPARATION 2B, and making non-critical variations to replace 1,3-benzodioxol-5-ol with 2,3-dihydrobenzofuran-5-ol, (Alabaster, R. J., et al.; Synthesis (1988), 12:950-2) and 1-(2-cyclopropylethyl)-1H-indole-2,3-dione with 1-(diphenylmethyl)-1H-indole-2,3-dione, the title compound was obtained: MS (ES+) m/z 472.2 (M+23).

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-1edc83fe48db4c7a8aeae15ed7f93fc3
来源数据集: uspto-grants-2012_01
DOI: 10.6084/m9.figshare.5104873.v1
专利: US08106087B2
来源说明: uspto-grants-2012_01

反应 SMILES

O1C2C=CC(O)=CC=2OC1.[O:11]1[C:15]2[CH:16]=[CH:17][C:18]([OH:20])=[CH:19][C:14]=2[CH2:13][CH2:12]1.C1(CCN2C3C(=CC=CC=3)C(=O)C2=O)CC1.[C:37]1([CH:43]([C:55]2[CH:60]=[CH:59][CH:58]=[CH:57][CH:56]=2)[N:44]2[C:52]3[C:47](=[CH:48][CH:49]=[CH:50][CH:51]=3)[C:46](=[O:53])[C:45]2=[O:54])[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=1>>[C:55]1([CH:43]([C:37]2[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=2)[N:44]2[C:52]3[C:47](=[CH:48][CH:49]=[CH:50][CH:51]=3)[C:46]([OH:53])([C:17]3[C:18]([OH:20])=[CH:19][C:14]4[CH2:13][CH2:12][O:11][C:15]=4[CH:16]=3)[C:45]2=[O:54])[CH:56]=[CH:57][CH:58]=[CH:59][CH:60]=1