HRID425550

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID68289

Sesamol

C7H6O3

结构：O=C1C(=O)N(C(c2ccccc2)c2ccccc2)c2ccccc21

HCID1969277

1-(diphenylmethyl)-1H-indole-2,3-dione

C21H15NO2

HCID21485219

未命名化合物

HCID65596570

1-(2-cyclopropylethyl)-1H-indole-2,3-dione

C13H13NO2

PRODUCTS

生成物

结构：CC1(C)COc2cc(O)c(C3(O)C(=O)N(C(c4ccccc4)c4ccccc4)c4ccccc43)cc21

HCID12004274

未命名化合物

PROCEDURE

实验过程

Following the procedure as described in PREPARATION 2B, and making non-critical variations to replace 1-(2-cyclopropylethyl)-1H-indole-2,3-dione with 1-(diphenylmethyl)-1H-indole-2,3-dione, and 1,3-benzodioxol-5-ol with 3,3-dimethyl-2,3-dihydro-1-benzofuran-6-ol, the title compound was obtained: MS (ES+) m/z 478.5 (M+1).

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-bd5adcd3115c401d9ad2bd9b06e318ec
来源数据集: uspto-grants-2012_01
DOI: 10.6084/m9.figshare.5104873.v1
专利: US08106087B2
来源说明: uspto-grants-2012_01

反应 SMILES

C1(CCN2C3C(=CC=CC=3)C(=O)C2=O)CC1.[C:17]1([CH:23]([C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)[N:24]2[C:32]3[C:27](=[CH:28][CH:29]=[CH:30][CH:31]=3)[C:26](=[O:33])[C:25]2=[O:34])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1.O1C2C=CC(O)=CC=2OC1.[CH3:51][C:52]1([CH3:62])[C:56]2[CH:57]=[CH:58][C:59]([OH:61])=[CH:60][C:55]=2[O:54][CH2:53]1>>[C:35]1([CH:23]([C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=2)[N:24]2[C:32]3[C:27](=[CH:28][CH:29]=[CH:30][CH:31]=3)[C:26]([OH:33])([C:58]3[C:59]([OH:61])=[CH:60][C:55]4[O:54][CH2:53][C:52]([CH3:62])([CH3:51])[C:56]=4[CH:57]=3)[C:25]2=[O:34])[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=1