Sesamol → HCID 12004407, compound

HRID 425582Notes

Reaction equation

[CH2:1]([N:6]1[C:14]2[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=2)[C:8](=[O:15])[C:7]1=[O:16])[CH2:2][CH2:3][CH2:4][CH3:5].O1C2C=CC(O)=CC=2OC1.[O:27]1[C:31]2[CH:32]=[C:33]([OH:36])[CH:34]=[CH:35][C:30]=2[CH2:29][CH2:28]1>>[OH:15][C:8]1([C:34]2[C:33]([OH:36])=[CH:32][C:31]3[O:27][CH2:28][CH2:29][C:30]=3[CH:35]=2)[C:9]2[C:14](=[CH:13][CH:12]=[CH:11][CH:10]=2)[N:6]([CH2:1][CH2:2][CH2:3][CH2:4][CH3:5])[C:7]1=[O:16]

Participants

Reactant 3

HCID 68289Sesamol

HCID 15810921-Pentyl-1H-indole-2,3-dione

HCID 122365402,3-Dihydro-1-benzofuran-6-ol

Product 1

HCID 12004407HCID 12004407, compound

Procedure

Following the procedure as described in PREPARATION 2B, and making non-critical variations to replace1-(2-cyclopropylethyl)-1H-indole-2,3-dione with 1-pentyl-1H-indole-2,3-dione, and 1,3-benzodioxol-5-ol with 2,3-dihydrobenzofuran-6-ol, the title compound was obtained (90%) as a white powder: MS (ES+) m/z 376.3 (M+23).

Sources & evidence

ORD record: ord-5f20b138014a46cb9d3e1bfa9b519740
Source dataset: uspto-grants-2012_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08106087B2

Reaction notes

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