HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66703722, compound → HCID 59411631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66703722 | HCID 66703722 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59411631 | HCID 59411631 | — |
Reaction Steps
A solution of (1S,2S,5R)-2-(benzylamino-methyl)-3-aza-bicyclo[3.3.0]-octane-3-carboxylic acid tert.-butyl ester (354 mg) in EtOH (17 mL) was treated with Pd/C 10% (141 mg) and stirred under hydrogen (1 bar) for 16 h. After filtration through celite and removal of the solvents the title compound was obtained as an oil which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08106215B2 |
| Source dataset | uspto-grants-2012_01 |
| ORD ID | ord-8a1ec0ba5b514935bd2a0caeaef055be |
| Source note | uspto-grants-2012_01 |