HCID 59411622, compound → HCID 59411620, compound

Participants

Reaction Steps

A solution of (1R,3aS,3bS,6aR)-5-methyl-1-phenyl-3a,3b,6,6a-tetrahydro-3H-2-oxa-7a-aza-cyclopenta[a]pentalen-7-one (Jao E. et al Tetrahedron Letters, 2003, 44, 5033-5035) (2.34 g) in EtOH (23 mL) was treated with Pd/C 10% (456 mg) and stirred under hydrogen (1 bar) for 1.5 h. After filtration through celite and removal of the solvents the title compound was obtained as an oil, which was used without further purification.

Provenance & Evidence