HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → 5-[2-(N,N-Dimethylamino)ethyl]-2-furanmethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N,N-Dimethyl-2-furanethanamine | HCID 38131 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 5-[2-(N,N-Dimethylamino)ethyl]-2-furanmethanol | HCID 23452109 | — |
Reaction Steps
N,N-Dimethyl-2-furanethanamine (9.8 g), 30% aqueous formaldehyde (17.5 g) and glacial acetic acid (18 ml) were heated at 70° for 5 hr. The reaction was cooled, basified with sodium hydroxide and extracted with ether. The organic extracts were distilled to give an oil b.p. 90°-100° (0.5 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04169855 |
| Source dataset | uspto-grants-1979_10 |
| ORD ID | ord-349503248c744d2e845687065abce6e7 |
| Source note | uspto-grants-1979_10 |