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HRID426571

反应详情

EQUATION

反应方程式

HRID 426571 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C(Cl)c1ccco1
HCID68242

2-Furancarbonyl chloride

C5H3ClO2

结构：CCCCCC(O)O
HCID147023

Hexanediol

C6H14O2

PRODUCTS

生成物

1
结构：CCCCCC(OC(=O)c1ccco1)OC(=O)c1ccco1
HCID54192328

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Furoyl chloride 121 g (0.93 m) added to 52 g (0.44 m) hexanediol, 133 g (1.3 m) triethylamine and 485 g methylene chloride at 5°-10°. Yield of 92 g recrystallized from isopropyl alchol, 69°-71° m.p.

WORKUP

后处理

  1. customYield of 92 g recrystallized from isopropyl alchol, 69°-71° m.p.