HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Furancarboxylic acid → 2-Butoxyethylfuroate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Furancarboxylic acid | HCID 6919 | — |
| Reactant | 2-Butoxyethanol | HCID 8133 | — |
| Reactant | Dibutyltin dioctanoate | HCID 16683953 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 2-Butoxyethylfuroate | HCID 86736659 | — |
Reaction Steps
2-Butoxyethanol (butyl cellosolve) 121 g (1.02 m), furoic acid 95 g (0.85 m) and 1 g dibutyltin dioctoate were heated with a xylene azeotrope to acid number 3. Xylene removed by distillation to a pot temperature of 200° and reaction product distilled. 2-Butoxyethylfuroate collected in fraction 2, 111°-104°. Yield 162 g, 86%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04170584 |
| Source dataset | uspto-grants-1979_10 |
| ORD ID | ord-a6942e00bb424faf850a7066f166f3c6 |
| Source note | uspto-grants-1979_10 |