Methyl iodide → HCID 178503966, compound

HRID 426735Notes

Reaction equation

HRID 426735 reaction equation
[C:1]1([N:7]2[C:11]([NH:12][C:13]([NH2:15])=[S:14])=[CH:10][C:9]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)=[N:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:22][I:23]>>[IH:23].[C:1]1([N:7]2[C:11]([NH:12][C:13](=[NH:15])[S:14][CH3:22])=[CH:10][C:9]([C:16]3[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=3)=[N:8]2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 12763850N-(1,3-Diphenyl-1H-pyrazol-5-yl)thiourea

Product 1

HCID 178503966HCID 178503966, compound

Procedure

(1,3-Diphenyl-5-pyrazolyl) thiourea (119.7 g.) and 63.9 g. methyl iodide were reacted as described in Example V to give 156.1 g. of product, mp 178°-182° C.

Workup

  1. customto give 156.1 g

Sources & evidence

ORD record
ord-5fbb17aee954471abf116bdb9ff5e0ac
Source dataset
uspto-grants-1979_10
Patent number
US04171367

Reaction notes

Loading…