HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-(2-Aminoethyl)-5-(2,4-dinitrophenylthio)tetrazole hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-(2-Acetamidoethyl)-5-(2,4-dinitrophenylthio)tetrazole | HCID 20382814 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(2-Aminoethyl)-5-(2,4-dinitrophenylthio)tetrazole hydrochloride | HCID 20382811 | — |
Reaction Steps
A mixture of 6.5 g (0.02 mol) of 1-(2-acetamidoethyl)-5-(2,4-dinitrophenylthio)tetrazole, 100 ml of 12 N hydrochloric acid and 100 ml of 95% ethanol was refluxed for 4.5 hours. The mixture was evaporated to dryness to give a gummy residue which crystallized upon addition of ethanol to give 1-(2-aminoethyl)-5-(2,4-dinitrophenylthio)tetrazole hydrochloride, mp 217°-219° (d).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04171368 |
| Source dataset | uspto-grants-1979_10 |
| ORD ID | ord-0e6df9c684e943968d248a1662f925f2 |
| Source note | uspto-grants-1979_10 |