HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 826790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Magnesium | HCID 5462224 | — |
| Reactant | HCID 20389855 | HCID 20389855 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 826790 | HCID 826790 | — |
Reaction Steps
From 4.9 g (0.2 mole) of magnesium, 31.2 g (0.2 mole) of ethyl iodide in abs. ether and 23.2 g (0.1 mole) of benzo[f]thieno[2,3-b]thiepin-4(5H)-one, there is obtained 4-ethyl-4,5-dihydro-benzo[f]thieno[2,3-b]thiepin-4-ol as an oily crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04171366 |
| Source dataset | uspto-grants-1979_10 |
| ORD ID | ord-d6e47e9cab5e4db28e3730dffb899354 |
| Source note | uspto-grants-1979_10 |