N-Methyltriimidodicarbonic acid → HCID 20476324, compound

HRID 426832Notes

Reaction equation

HRID 426832 reaction equation
[CH2:1]([NH:5][C:6]([NH:8][C:9]([NH2:11])=[O:10])=[O:7])[CH2:2][CH2:3][CH3:4].[CH3:12]NC(NC(N)=O)=O>>[CH2:1]([N:5]1[CH:12]=[N:11][C:9](=[O:10])[NH:8][C:6]1=[O:7])[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 231880N-Methyltriimidodicarbonic acidHCID 4360848Imidodicarbonic diamide, N-butyl-

Product 1

HCID 20476324HCID 20476324, compoundYield 92%

Procedure

Following the procedure described in Preparation 2, Part B, above, but substituting the n-butylbiuret prepared in Part A, above, for the methylbiuret, there is prepared 60 gm. (92% yield) of 1-n-butyl-5-azauracil.

Workup

  1. customdescribed in Preparation 2, Part B
  2. customprepared in Part A

Sources & evidence

ORD record
ord-2b388ab6cb604defbe463978c0514581
Source dataset
uspto-grants-1979_10
Patent number
US04171431

Reaction notes

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