2,5-Dimethyl-3-nitrophenol → 1-Acetyl-4-benzyloxy-6-methyl-indazole

HRID 426837Notes

Reaction equation

HRID 426837 reaction equation
[NH:1]([C:5]1[C:6]([CH3:20])=[C:7]([O:12][CH2:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH:8]=[C:9]([CH3:11])[CH:10]=1)[C:2]([CH3:4])=[O:3].CC1C([N+:28]([O-])=O)=CC(C)=CC=1O>>[C:2]([N:1]1[C:5]2[C:6](=[C:7]([O:12][CH2:13][C:14]3[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=3)[CH:8]=[C:9]([CH3:11])[CH:10]=2)[CH:20]=[N:28]1)(=[O:3])[CH3:4]

Participants

3

Reactant 2

HCID 189815232,5-Dimethyl-3-nitrophenolHCID 70601315(3-Acetamino-2,5-dimethyl-phenyl)-benzyl ether

Product 1

HCID 203901821-Acetyl-4-benzyloxy-6-methyl-indazole

Procedure

The (3-acetamino-2,5-dimethyl-phenyl)-benzyl ether used as starting material in Example 2 is prepared from 2,5-dimethyl-3-nitrophenol by the following reactions:

Sources & evidence

ORD record
ord-d78bbe6c15734f1a926bef42c82c0c47
Source dataset
uspto-grants-1979_10
Patent number
US04171446

Reaction notes

Loading…