HCID 20390178, compound → HCID 20390187, compound

HRID 426841Notes

Reaction equation

HRID 426841 reaction equation
C(N1C2C(=C(OCC3OC3)C(C)=CC=2)C=N1)(=O)C.C(N1C2C(=C(OCC3OC3)C=CC=2C)C=N1)(=O)C.[C:37]([N:40]1[C:48]2[C:43](=[C:44]([O:51][CH2:52][CH:53]3[O:55][CH2:54]3)[CH:45]=[C:46]([CH2:49]C)[CH:47]=2)[CH:42]=[N:41]1)(=[O:39])[CH3:38]>>[C:37]([N:40]1[C:48]2[C:43](=[C:44]([O:51][CH2:52][CH:53]3[O:55][CH2:54]3)[CH:45]=[C:46]([CH3:49])[CH:47]=2)[CH:42]=[N:41]1)(=[O:39])[CH3:38]

Participants

4

Reactant 3

HCID 20390178HCID 20390178, compoundHCID 20390204HCID 20390204, compoundHCID 20390214HCID 20390214, compound

Product 1

HCID 20390187HCID 20390187, compound

Procedure

The following compounds are obtained in an analogous manner: 1-acetyl-4-(2,3-epoxypropoxy)-5-methyl-indazole (m.p. 75°-76° C.), 1-acetyl-4-(2,3-epoxypropoxy)-7-methyl-indazole (m.p. 108°-109° C.) and 1-acetyl-4-(2,3-epoxypropoxy)-6-ethylindazole (m.p. 77°-78° C.).

Workup

  1. customThe following compounds are obtained in an analogous manner

Sources & evidence

ORD record
ord-8044ef2a858e4a4e94b5fd668f20f64a
Source dataset
uspto-grants-1979_10
Patent number
US04171446

Reaction notes

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