HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus tribromide → HCID 54251209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | Lithium Bromide | HCID 82050 | — |
| Reactant | HCID 23455710 | HCID 23455710 | — |
| Catalyst | Zinc bromide | HCID 10421208 | — |
| Product | HCID 54251209 | HCID 54251209 | — |
Reaction Steps
6-(3,4-Methylenedioxyphenyl)-3-hexenyl bromide [V; Ar is 3,4-methylenedioxyphenyl, R is H] was prepared from 11.5 g. of 2-(3,4-methylenedioxyphenyl)ethyl cyclopropyl carbinol (Preparation B2), 12 g. of phosphorus tribromide, 10 g. of lithium bromide and 12.7 g. of zinc bromide according to the procedure given above in Preparation C1, affording 12.5 g. of product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04171378 |
| Source dataset | uspto-grants-1979_10 |
| ORD ID | ord-51c59e9f49154c1d936b600a5892856d |
| Source note | uspto-grants-1979_10 |