HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus tribromide → HCID 53838392, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | Lithium Bromide | HCID 82050 | — |
| Reactant | HCID 23455750 | HCID 23455750 | — |
| Catalyst | Zinc bromide | HCID 10421208 | — |
| Product | HCID 53838392 | HCID 53838392 | — |
Reaction Steps
6-(4-Methoxyphenyl)-3-hexenyl bromide [V; Ar is 4-CH3OC6H4, R is H] was prepared from 38.2 g. of 2-(4-methoxyphenyl)ethyl cyclopropyl carbinol (Preparation B5), 42.5 g of phosphorus tribromide, 35 g. of lithium bromide and 40 g. of zinc bromide according to the procedure given above in Preparation C1, affording 48 g of product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04171378 |
| Source dataset | uspto-grants-1979_10 |
| ORD ID | ord-c38d99278ff544c8b124b732e52977fb |
| Source note | uspto-grants-1979_10 |