HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 58484330, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 6-Chloro-5-formyl-1,3-dimethyluracil | HCID 319971 | — |
| Product | HCID 58484330 | HCID 58484330 | — |
Reaction Steps
The process described in Method C was followed. 6-Chloro-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carbaldehyde (0.270 g, 1.33 mmol) and methanol were used to obtain the title compound. The crude product was purified by column chromatography with a mixture of n-hexane:ethyl acetate (4:1) as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08536210B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-c85dff6070af47f89ad63f95a7464379 |
| Source note | uspto-grants-2013_09 |