Methanol → HCID 54482457, compound

HRID 426938Notes

Reaction equation

HRID 426938 reaction equation
[CH3:1][N:2]1[CH:6]=[C:5]([CH:7]=[CH:8][C:9](Cl)=[O:10])[C:4]([N+:12]([O-:14])=[O:13])=[N:3]1.[CH3:15][OH:16]>>[CH3:1][N:2]1[CH:6]=[C:5]([CH:7]=[CH:8][C:9]([O:16][CH3:15])=[O:10])[C:4]([N+:12]([O-:14])=[O:13])=[N:3]1

Participants

3

Reactant 2

HCID 887MethanolHCID 54231082HCID 54231082, compound

Product 1

HCID 54482457HCID 54482457, compound

Procedure

The same product is obtained when 0.22 g. of the 3-(1-methyl-3-nitro-4-pyrazolyl)-acrylic acid chloride described in Example 2 is allowed to react in 1.8 ml. methanol for 30 minutes at ambient temperature and the resultant crystals filtered off with suction.

Workup

  1. customThe same product is obtained when 0.22 g
  2. customto react in 1.8 ml
  3. filtrationthe resultant crystals filtered off with suction

Sources & evidence

ORD record
ord-ebec430c206148b79bfc7e723acc2de8
Source dataset
uspto-grants-1979_10
Patent number
US04172136

Reaction notes

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