HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Pentanoyl chloride, 4-methyl- → 2-(4-Methyl-1-oxopentyl)furan
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Pentanoyl chloride, 4-methyl- | HCID 170008 | — |
| Edukt | 2-(Tributylstannyl)furan | HCID 4393688 | — |
| Katalysator | HCID 178418476 | HCID 178418476 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | 2-(4-Methyl-1-oxopentyl)furan | HCID 95287 | — |
Reaktionsschritte
A solution of 2-tributylstannylfuran (1 mmol), 4-methylvaleroyl chloride (1.1 mmol), and PdCl2(PPh3)2 (0.05 mmol) in THF was stirred at 25° C. for 24 h. Extraction and chromatography gave 2-(4-methylvaleryl)furan.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06312662B1 |
| Quelldatensatz | uspto-grants-2001_11 |
| ORD ID | ord-4b7281dd45df4ecebc4c09ab97e8a6b1 |
| Quellennotiz | uspto-grants-2001_11 |